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The pressure of one’s reactor chamber try step one,600 Pa, and the electricity out of progress is actually 2,2 hundred W (the new voltage are ∼20 V, and the newest try ∼120 A great). The development energy of your first collection is set while the step one,800 W, and also the gains day is determined since the 0, 31, 60, 90, 120, 180, and you will 210 s. The fresh test labels try 0-s, 30-s, 60-s, 90-s, 120-s, 180-s, and 210-s, respectively. Another group of examples had a rise power of 1,600 W to advance sluggish the organization speed and you can prolong the new growth time for you to showcase the growth procedure for the movies. The growth time is decided lengthened since the dos, cuatro, six, 8, ten, and you may a dozen minute, plus the sample labels is dos-minute, 4-minute, 6-minute, 8-minute, 10-min and you may a dozen-min, respectively.
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Quicker dust in the nanometer size are faultless, however, huge of these of numerous 10s of nanometers produce crystal faults. Destruction of one’s diamond seeds crystals considering the electron ray irradiation is talked about in terms of manufacturing from diamond film. Also, the growth cycle lower than 1,600 W is actually ∼4 min, more than ∼90 s less than step 1,800 W, showing one a minimal growth strength of just one,600 W actually decreases the growth rate and you can stretches the organization cycle. The brand new 0-s try displays an average Raman functions from NCD video (26).
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It is extremely experienced a great multifunctional issue and draws far attention. Yet not, it is rather tough to prepare yourself higher-city expensive diamonds, that is a shield on the application. Experts have developed different ways, in addition to large-tension high-heat (HPHT) and you may chemical compounds steam deposition (CVD) to prepare unmarried crystals, microcrystallines, and nanocrystalline diamonds (1–5).
۱A shows a regular cauliflower-such as morphology from particles to your SPF flick (recognized as 0-s sample). A huge number of vertical-broadening sheets molded because the progress date increased to 30 s (Fig. 1B, called 30-s try), and became big at the 60 s (Fig. 1C, called sixty-s try). Nevertheless, these types of sheets disappear within the 90 s (Fig. 1D, titled 90-s test), proving hairless cauliflower-including dust once again.
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